Natrolite - Sample 2 NanED Round Robin, Data: ESR8 & ESR9

Description

Natrolite The following submission contains the data collection and processing for the sample natrolite under the NanEd round-robin project.  Precession Electron Diffraction (PED) was used to collect the dataset on the target crystal.  The dataset was processed with PETS2 and eADT software. The table below summarizes the data collection parameters for the dataset.   General information:   Project NanED (www.naned.eu) ESR Project ESR8 & ESR9 - Round Robin Project Label RR2 Sample Label RR2-S2_ PRAHA Data set Label RR2_Cry2     Instrumental:   Instrument FEI TECNAI F30 STWIN Radiation source FEG Accelerating voltage 300 kV Wavelength 0.0197 Å Probe Type Nanodiffraction Beam Diameter 200nm Beam Convergence Semi-parallel beam Detector US4000 - CCD camera GATAN (16-bit) (bottom mounted) Number of pixels in the image 2048 x 2048 Pixel size 15 µm x 15 µm Camera Length / Effective Camera Length 750 mm / 702 mm Calibration constant (not corrected for Effective Camera length) 0.00152 Å-1/pixel  Hardware Binning 2  Sample description:   Name Natrolite Chemical composition Na2Al2Si3O10·2H2O Sample source Natural sample from Marianska Skala, Usti nad Labem, Czechia Sample preparation The crystals were grinded in an agata mortar and part of the resulting powder was loaded on the carbon side of a carbon-coated copper grid (300 mesh). Experimental:   Data Type Electron diffraction data - 3D ED Data collection method Precession Temperature (K) used during data collection 293 K Number of crystals contributing to the data set 1 Number of experimental frames 131 tilt range, tilt step, tilt per frame -65° to +65°, 1°, 0° Precession angle 1° Exposure time per frame 250 ms     Software:   Software used for the data collection Gatan Digital Micrograph software Software used for processing PETS2 and eADT     Authorship and bibliography   Author(s) of the data Laura Gemmrich Hernández (ESR8) & Marco Santucci (ESR9) Related data   Publication(s)       Files and data formats   Image folder img: Folder containing images of the diffraction pattern from each frame. Image format tiff_16bit_unsigned          

Resources

Name Format Description Link
0 http://data.europa.eu/88u/dataset/oai-zenodo-org-7543857
0 http://data.europa.eu/88u/dataset/oai-zenodo-org-7543857

Tags

  • naned
  • precession-electron-diffraction
  • natrolite
  • 3ded

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