Supporting data for manuscript describing Slice and Dice method to measure NMR relaxation with nested experiments

Description

This is a supporting dataset for the manuscript "Slice and Dice: Nested Spin-lattice Relaxation Measurements" by W. Trent Franks, Jacqueline Tognetti and Józef R. Lewandowski. NMR_data.zip : Raw NMR data in the Bruker format for the experiments presented in the manuscript. The file expands to a directory called "Raw NMR Data" that contains: ReadMe_NMR_data.txt - describing the datasets included in the file. Record 1: 13C\(^\alpha\) individual experiment. Pulse program name: hRCH_CT1 Record 2: 13C' individual experiment. Pulse program name: hCOcaH_SP_T1 Record 3: 15N individual experiment. Pulse program name: hRNH_NT1b Record 10: 13C\(^\alpha\) + 13C' + 15N Slice & Dice experiment. Pulse program name: hR[COca,Ca,N]Ha_T10818 corresponding to the final sequence: hR[N,COca,Ca]HR_T1 Pulse_program.zip: The pulse program and include file for the Slice and Dice experiment described in the manuscript. The pulse program in Bruker format (war.hR[COca,Ca,N]H_T1 - this is a text file that can be opened with any text editor) was tested on a Bruker Avance III HD console. Both the pulse program file, war.hR[COca,Ca,N]H_T1, and include file, HCN_defs.incl, need to be placed in the pulse program directory (/opt/topspinXX/exp/stan/nmr/lists/pp/user where XX is replaced with the version of Topspin). The file expands to a directory "Pulse_program_incl" that contains: war.hR[COca,Ca,N]H_T1 - pulse program HCN_defs.incl - include file ReadMe_SliceDice_pp.txt - details on how to set up the experiment. HowToProcess_SliceDice.txt: Instructions on how to process Slice and Dice experiment in Topspin. MultiR1list.zip: A program written in Python 3 required to calculate delay lists for the nested experiment to be included in the pulse program. The file expands to a directory MultiT1list directory that contains: MultiT1list.py - the program ReadMe_MultiT1list.txt - instructions on how to use the program    

Resources

Name Format Description Link
0 http://data.europa.eu/88u/dataset/oai-zenodo-org-5965023

Tags

  • pulse-program
  • nmr
  • methodology
  • accelerated-acquistion
  • solid-state-nmr
  • protein-dynamics
  • spin-lattice-relaxation
  • magic-angle-spinning
  • nested-experiments

Topics

Categories