AM Bench 2022 Microstructure Measurements for IN718 3D builds

The following data files include microstructure measurement results associated with the 2022 Additive Manufacturing Benchmark test series (AM-Bench 2022) AMB2022-01 benchmark on laser powder bed fusion (LPBF) 3D builds of nickel-based superalloy IN718 test objects. The AM builds were performed on the NIST Additive Manufacturing Metrology Testbed (AMMT) and the microstructure measurements were conducted using scanning electron microscopy (SEM), transmission electron microscopy (TEM), ultra-small-angle X-ray scattering (USAXS), small-angle X-ray scattering (SAXS), wide-angle X-ray scattering (WAXS), and automated serial sectioning. Detailed descriptions of the build process parameters, scan pattern, heat treatment, and descriptions of all of the AMB2022-01 measurements are provided on the AMB2022-01 challenge description webpage (https://www.nist.gov/ambench/amb2022-01-benchmark-measurements-and-challenge-problems).Due to the time-sensitive nature of the AM Bench challenge problems, those measurements and analyses were prioritized. The challenges that this data publication address are:Microstructure (CHAL-AMB2022-01-MS): Histograms of direction-specific grain sizes from specified regions within as-built and heat-treated samples.Phase Evolution (CHAL-AMB2022-01-PE): Formation and evolution of phases and phase fractions, including major precipitates, as a function of time for heat treatments of IN718 from a 2.5 mm leg.The data provided for CHAL-AMB2022-01-PE are preliminary since an additional phase in the as-build material has not yet been positively identified. These data will be updated shortly. Also, additional datasets that are not required for the challenges will be added soon. For updates, please check back here or at www.nist.gov/ambench.